Merseyside Police said more than 30 canisters of nitrous oxide were found in a car in the early hours of 25 November.
Two boys, aged 15 and 16, and a man, 30, were arrested on suspicion of possession of a psychoactive substance with intent to supply after a Ford Kuga car was stopped in Sefton Street.
Det Insp Steve Byrom said: “Abuse of nitrous oxide is dangerous and is often linked to antisocial behaviour and criminality.
“We would encourage people to think about the possible consequences of possessing or selling this illegal drug.”
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