Ayling was part of the Leeds squad that won promotion to the Premier League under Marcelo Bielsa in 2020.
But he lost his place during last season and went to Middlesbrough on loan.
He leaves Elland Road having played 268 games and scored 11 goals following his move from Bristol City eight years ago.
Carrick said he was delighted to have him on board as the Teesside club’s first transfer of the summer.
“After coming in on loan in January, Luke settled in very quickly and made a big impact, bringing his character and personality to the group,” Carrick told the club’s website, external.
“He knows what it takes to be a success in this league.”
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